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      Raw data for new compounds described in the paper: "Enantioselective nickel-catalyzed arylative intramolecular 1,4-allylations"

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      HWL_Nickel-catalyzed intramolecular 1,4-allylations_raw data.zip (368.6Mb)
      Publication date
      2018-05-14
      Creators
      Lam, Hon Wai
      Metadata
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      Description
      Raw data for new compounds described in the paper: "Enantioselective nickel-catalyzed arylative intramolecular 1,4-allylations" The enantioselective nickel-catalyzed desymmetrization of allenyl cyclohexa-2,5-dienones by reaction with arylboronic acids is described. Nickel-catalyzed arylation of the allene gives allylnickel species, which undergo cyclization by 1,4-allylation to produce hexahydroindol-5-ones and hexahydrofuran-5-ones with three contiguous stereocenters in high diastereo- and enantioselectivities.
      External URI
      • https://rdmc.nottingham.ac.uk/handle/internal/358
      DOI
      • http://doi.org/10.17639/nott.354
      Related publication DOI
      • 10.1039/C8CC03204A
      Subjects
      • Chemicals
      • Enantioselective catalysis
      • Arylation
      • Allenes
      • Raw data for new compounds described in the paper: "Enantioselective nickel-catalyzed arylative intramolecular 1,4-allylations"
      • Physical sciences::Chemistry::Organic chemistry::Organometallic chemistry
      • Q Science::QD Chemistry::QD241 Organic chemistry
      Divisions
      • University of Nottingham, UK Campus::Faculty of Science::School of Chemistry
      Deposit date
      2018-05-14
      Data type
      IR, NMR, mass spectrometry, and HPLC data
      Contributors
      • Nguyen, Thi Le Nhon
      • Incerti-Pradillos, Celia
      • Lewis, William
      Funders
      • Other
      • University of Nottingham
      • GlaxoSmithKline
      Data collection method
      Using IR, NMR, and mass spectrometers, and HPLC machines
      Resource languages
      • en
      Publisher
      Royal Society of Chemistry

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