Data for yield, characterisation and electrochemical performance measurements of sodium carboxylates

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Publication date
2024-12-30
Creators
Laybourn, Andrea
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Description
This research involves the synthesis of disodium terephthalate and disodium napthalates. These materials have potential application as sodium anodes in batteries. Data collected informed conditions relevant to optimisation based on yield, textural properties, and electrochemical performance. This includes: data files for synthesis conditions (microwave energy, yield), characterisation (PXRD, FTIR, ICP-MS, TGA and SEM images) and half and full cell electrochemical performances.
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DOI
Subjects
  • Sodium ion batteries
  • Anodes
  • Environmental impact analysis
  • Sodium-Ion Batteries, Organic Anodes, Microwave-Assisted Synthesis, Environmental Impact Assessment, LCA
  • Physical sciences
  • Technologies
  • TK Electrical engineering. Electronics Nuclear engineering
Divisions
  • University of Nottingham, UK Campus::Faculty of Engineering::Department of Chemical and Environmental Engineering
Research institutes and centres
  • University of Nottingham, UK Campus
Deposit date
2024-12-17
Corporate creators
  • Faradion Limited
Data type
Raw datasets in excel: electrochemical characterisation, ICP-MS, PXRD, FTIR, TGA, MW energy information, yield. Also SEM images.
Contributors
  • Puscalau, Constantin
  • Desai, Aamod V.
  • Lizundia, Erlantz
  • Ettlinger, Romy
  • Adam, Mohamed
  • Morris, Russell
  • Armstrong, A. Robert
  • Tokay, Begum
Funders
  • Engineering & Physical Sciences Research Council
  • Faraday Institution
  • European Research Council
  • Engineering and Physical Sciences Research Council (EPSRC) and Science Foundation Ireland (SFI) Centre for Doctoral Training in Sustainable Chemistry: Atoms-2-Products an Integrated Approach to Sustainable Chemistry
  • University of the Basque Country
Grant number
  • FIRG018
  • FIRG064
  • 787073
  • EP/T019298/1
  • EP/R023751/1
  • EP/S022236/1
  • EP/L022494/1
  • GIU21/010
Collection dates
  • October 2021 to December 2024
Data collection method
Microwave data: Sairem MiniFlow 200SS (Sairem, Neyron, France); Powder X-ray diffraction (PXRD) Bruker D8 Advance DaVinci, software Profex 5.0 and Mercury 4.1.3; Fourier-transform infrared (FT-IR) spectra Bruker platinum alpha FTIR spectrometer, OPUS 5.5 software; TGA TA Instruments TGA 550; SEM images of all materials were recorded on a JEOL JSM-IT800 microscope; ICP-MS (Thermo-Fisher Scientific iCAP-Q; Thermo Fisher Scientific, Bremen, Germany) software used Qtegra™ software (Thermo-Fisher Scientific); electrochemical testing performed using Biologic BCS-805 modular battery testing system or a Neware BTS tester, data analysis using BT-Lab or BTSDA software; life cycle assessment (LCA) methodology as set by the ISO 14040/44 international standards, cradle-to-gate system boundary assessment was conducted using the OpenLCA 2.1.1 software and the ecoinvent v3.10 cut-off processes database, environmental impacts were determined using the ReCiPe 2016 Midpoint (H) methodology.
Legal and ethical issues
Do not process or publish data without consent
Provenance / lineage
Paper, title: Rapid Gram-Scale Microwave-Assisted Synthesis of Organic Anodes for Sodium-Ion Batteries with Environmental Impact Assessment
Resource languages
  • en
Copyright
  • Andrea Laybourn
  • Russell E. Morris
  • A. Robert Armstrong
Publisher
The University of Nottingham
CC-BY
Except where otherwise noted, this item's license is described as Creative Commons by Attribution