Data for yield and characterisation and performance measurements of UTSA-16 magnetic framework composites synthesised in flow

Thumbnail
View/Open
Publication date
2024-10-02
Creators
Laybourn, Andrea
Metadata
Show full item record
Description
Data collected herein support the following article and supplementary information: Continuous flow synthesis of MOF UTSA-16(Zn), mixed-metal and magnetic composites for CO2 capture – toward scalable manufacture. Data include: yield and temperature for decomposition (TGA), carbon dioxide adsorption and capture-release cycling (TGA), gas sorption isotherms, mineral liberation analysis, vibrating sample magnetometry, induction heating profiles, scanning electron microscopy (SEM) images, and inductively coupled plasma optical emission spectroscopy (ICP-OES), x-ray diffraction and lab book notes.
External URI
DOI
Links
Subjects
  • Microscopy
  • Electron microscopy
  • Thermogravimetry
  • Diffraction
  • Inductively coupled plasma spectrometry
  • UTSA-16, magnetic framework composites, magnetic induction swing adsorption, scanning electron microscopy images, heating profiles, gas sorption data, lab book notes, thermogravimetric analysis data, vibrating sample magnetometry data, powder x-ray diffraction, yields, mineral liberation analysis images, inductively coupled plasma optical emission spectra (ICP-OES), gravimetric carbon dioxide sorption data
  • Engineering::Chemical, process & energy engineering
  • T Technology::TP Chemical technology
Divisions
  • University of Nottingham, UK Campus::Faculty of Engineering::Department of Chemical and Environmental Engineering
Research institutes and centres
  • University of Nottingham, UK Campus
Deposit date
2024-10-02
Corporate creators
  • Royce Discovery Centre, The University of Sheffield
  • Department of Chemistry and Materials Innovation Factory, University of Liverpool
  • University of Nottingham
Data type
scanning electron microscopy images, heating profiles, gas sorption data, lab book notes, thermogravimetric analysis data, vibrating sample magnetometry data, powder x-ray diffraction, yields, mineral liberation analysis images, inductively coupled plasma optical emission spectra (ICP-OES), gravimetric carbon dioxide sorption data.
Contributors
  • Woodliffe, John Luke
  • Molinar-Díaz, Jesús
  • Clowes, Rob
  • Hussein, Oday H.
  • Lester, Ed
  • Ferrari, Rebecca
  • Ahmed, Ifty
  • Johnston, Amy-Louise
  • Archibald, Vikki
Funders
  • Engineering & Physical Sciences Research Council
  • Other
  • Science Foundation Ireland
Grant number
  • Royce Discovery Centre, University of Sheffield; EPSRC Grant Number EP/R00661X/1 & EP/P02470X/1
  • Engineering and Physical Sciences Research Council (EPSRC) and Science Foundation Ireland (SFI) Centre for Doctoral Training in Sustainable Chemistry: Atoms-2-Products an Integrated Approach to Sustainable Chemistry, Grant number: EP/S022236/1
  • SEM analyses were supported by the EPSRC (EP/L022494/1) and the University of Nottingham
  • MLA/EDS analyses were supported by the EPSRC (EP/P006701/1), as part of the “EPSRC Future Composites Manufacturing Research Hub”
Parent project
  • https://eprints.nottingham.ac.uk/76979/
  • Magnetic framework composites for CO2 capture John Luke Woodliffe PhD project
Collection dates
  • September 2020 - July 2024
Coverage
  • UK
Data collection method
powder x-ray data: Bruker D8 Advance DaVinci with a Lynxeye 1D detector (Bragg-Brentano geometry), SEM images: Jeol 7000F FEG-SEM (Jeol PC-SEM software), MLA: Backscattered electron (BSE) imaging and chemical analyses using SEM, FEI Quanta600 based mineral liberation analysis (MLA) equipped with energy dispersive X-ray spectroscopy (EDS) for compositional analysis and linked Bruker/JKTech/FEI data acquisition software for automated mineralogy, TGA data: TA instruments TGA550 Discovery, gravimetric CO2 capture release cycles: TA instruments TGA550 Discovery, N2 and CO2 isotherms: Micromeritics ASAP 2020 V4.04, Vibrating-sample magnetometry (VSM): Quantum Design SQUID MPMS3, heating profiles: Cheltenham Induction Heating Ltd induction heater (2 kW, 204 kHz), Inductively coupled plasma optical emission spectroscopy (ICP-OES) Agilent 5110 Vertical Dual View instrument equipped with 240 place SPS-4 autosampler instrument operation and data processing was via the Agilent ‘ICP Expert’ software package.
Legal and ethical issues
Do not process or publish data without consent
Resource languages
  • en
Copyright
  • Andrea Laybourn
  • John Luke Woodliffe
Publisher
The University of Nottingham
CC-BY
Except where otherwise noted, this item's license is described as Creative Commons by Attribution