% Data for paper:
% S.J. Attwood, D. Leech, Y. He, A. Croft, R. J.M. Hague, D.J. Irvine, R.D. Wildman, A. Pordea, 
% High resolution 3D printed biocatalytic reactor core with optimized efficiency for continuous flow synthesis, 
% Chemical Engineering Science (2024).

%Info
% t24p24 means core with 24um thickness walls, 24um channels
% Each data set has an associated date (eg'20211022') and reactor core (eg 't24p24')
% followed by three replicates of absorbance taken at 420nm, followed by three blank samples
% See manuscript for more information 

%*Parameters*
% Params = 
% 1 - Volume of Print (ul)
% 2 - total volume test solution (ml)
% 3 - experiment time (min)
% 4 - total well volume (ul)
% 5 - sampled volume (ul)
% 6 - molecular weight ONP (mole/g)

%space occupied volume look up table
SOVTable = {'t12p24' 7.9; 't24p24' 7.9; 't48p24' 7.9; 't96p24' 6.82; 't216p24' 6.82; 't480p24' 7.9; 't24p48' 7.62; 't24p96' 7.35; 'L1250' 1.9531; 'L1500' 3.375; 'L1750' 5.3594; 'L2000' 8;};%mm3

%calibration 
Cal_1  = [2.6157 0.0105];%gradient and intercept data from 20220405

%STATIC DATA
%20211022 exp2
Data{n}={'20211022' 't24p24' 0.2276 0.2518 0.2745; '20211022' 'blank' 0.0495 0.0502 0.0499};
Params(n,:) = [5.9756 0.5 10 200 150 139];
Data{n}={'20211022' 't48p24' 0.2405 0.2495 0.2826; '20211022' 'blank' 0.0495 0.0502 0.0499};
Params(n,:) = [7.0679 0.5 10 200 150 139];
%20211022 exp3
Data{n}={'20211022' 't96p24' 0.1936 0.2125 0.2275; '20211022' 'blank' 0.0531 0.0509 0.0528};
Params(n,:) = [6.57 0.5 10 200 150 139];
Data{n}={'20211022' 't216p24' 0.208 0.2206 0.2332; '20211022' 'blank' 0.0531 0.0509 0.0528};
Params(n,:) = [6.7623 0.5 10 200 150 139];
%20211022 exp4
Data{n}={'20211022' 't480p24' 0.2344 0.242 0.2561; '20211022' 'blank' 0.0501 0.051 0.0518};
Params(n,:) = [7.8941 0.5 10 200 150 139];
Data{n}={'20211022' 't24p48' 0.2093 0.2181 0.2241; '20211022' 'blank' 0.0501 0.051 0.0518};
Params(n,:) = [4.3166 0.5 10 200 150 139];
%20211022 exp5
Data{n}={'20211022' 't24p96' 0.1498 0.1578 0.1693; '20211022' 'blank' 0.0505 0.0505 0.0502};
Params(n,:) = [2.7602 0.5 10 200 150 139];
%2021103 exp2
Data{n}={'20211103' 't24p24' 0.2299 0.2563 0.2621; '20211022' 'blank' 0.0583 0.0623 0.0613};
Params(n,:) = [5.9759 0.5 10 200 150 139];
Data{n}={'20211103' 't48p24' 0.262 0.2717 0.2882; '20211022' 'blank' 0.0583 0.0623 0.0613};
Params(n,:) = [7.0679 0.5 10 200 150 139];
% %2021103 exp4
Data{n}={'20211103' 't480p24' 0.2615 0.2805 0.2893; '20211022' 'blank' 0.0633 0.0618 0.0635};
Params(n,:) = [7.8941 0.5 10 200 150 139];
Data{n}={'20211103' 't24p48' 0.2074 0.2194 0.241; '20211022' 'blank' 0.0633 0.0618 0.0635};
Params(n,:) = [4.3166 0.5 10 200 150 139];
%2021110 exp2
Data{n}={'20211110' 't24p96' 0.161 0.165 0.1732; '20211022' 'blank' 0.0533 0.0537 0.055};
Params(n,:) = [2.7602 0.5 10 200 150 139];
Data{n}={'20211110' 't24p48' 0.2014 0.2131 0.2266; '20211022' 'blank' 0.0533 0.0537 0.055};
Params(n,:) = [4.3166 0.5 10 200 150 139];
%2021110 exp3
Data{n}={'20211110' 't24p24' 0.2439 0.2577 0.2824; '20211022' 'blank' 0.0549 0.054 0.0564};
Params(n,:) = [5.9756 0.5 10 200 150 139];
Data{n}={'20211110' 't48p24' 0.2242 0.233 0.2515; '20211022' 'blank' 0.0549 0.054 0.0564};
Params(n,:) = [7.0679 0.5 10 200 150 139];
%2021110 exp4
Data{n}={'20211110' 't96p24' 0.2136 0.235 0.2274; '20211022' 'blank' 0.0612 0.0595 0.0565};
Params(n,:) = [6.57 0.5 10 200 150 139];
Data{n}={'20211110' 't216p24' 0.2292 0.2433 0.2546; '20211022' 'blank' 0.0612 0.0595 0.0565};
Params(n,:) = [6.7623 0.5 10 200 150 139];
%2021110 exp5
Data{n}={'20211110' 't480p24' 0.2028 0.2187 0.2283; '20211022' 'blank' 0.0566 0.0568 0.0574};
Params(n,:) = [7.8941 0.5 10 200 150 139];
Data{n}={'20211116' 'L2000' 0.2579 0.2767 0.3035; '20211022' 'blank' 0.0514 0.0521 0.0676};
Params(n,:) = [8 0.5 10 200 150 139];
%2021116 exp3
Data{n}={'20211116' 'L1750' 0.1766 0.1876 0.2001; '20211022' 'blank' 0.0525 0.0533 0.0507};
Params(n,:) = [5.3594 0.5 10 200 150 139];
Data{n}={'20211116' 'L1500' 0.1815 0.1913 0.1993; '20211022' 'blank' 0.0525 0.0533 0.0507};
Params(n,:) = [3.375 0.5 10 200 150 139];
%2021116 exp4
Data{n}={'20211116' 'L1250' 0.1228 0.1349 0.1369; '20211022' 'blank' 0.0512 0.0555 0.0531};
Params(n,:) = [1.9531 0.5 10 200 150 139];
Data{n}={'20211116' 't480p24' 0.2068 0.2306 0.2391; '20211022' 'blank' 0.0512 0.0555 0.0531};
Params(n,:) = [7.8941 0.5 10 200 150 139];
%2021116 exp5
Data{n}={'20211116' 't216p24' 0.1983 0.2024 0.22; '20211022' 'blank' 0.0531 0.0538 0.0582};
Params(n,:) = [6.7623 0.5 10 200 150 139];
%20211203 exp2
Data{n}={'20211203' 'L2000' 0.2393 0.247 0.2695; '20211022' 'blank' 0.0557 0.0533 0.0528};
Params(n,:) = [8 0.5 10 200 150 139];
%20211203 exp3
Data{n}={'20211203' 'L1750' 0.1947 0.2059 0.2235; '20211022' 'blank' 0.0558 0.0571 0.0551};
Params(n,:) = [5.3594 0.5 10 200 150 139];
Data{n}={'20211203' 'L1500' 0.1632 0.1708 0.1766; '20211022' 'blank' 0.0558 0.0571 0.0551};
Params(n,:) = [3.375 0.5 10 200 150 139];
%20211203 exp4
Data{n}={'20211203' 'L1250' 0.1376 0.1486 0.1556; '20211022' 'blank' 0.051 0.0506 0.0527};
Params(n,:) = [1.9531 0.5 10 200 150 139];
Data{n}={'20211203' 't96p24' 0.218 0.2431 0.2439; '20211022' 'blank' 0.051 0.0506 0.0527};
Params(n,:) = [6.57 0.5 10 200 150 139];
% 20221109 exp1a
Data{n}={'20221109' 'L1250' 0.1267 0.124 0.1342; '20221109' 'blank' 0.0598 0.0579 0.0533};
Params(n,:) = [1.9531 0.5 10 200 150 139];
% 20221109 exp1b
Data{n}={'20221109' 'L1500' 0.1398 0.1527 0.1689; '20221109' 'blank' 0.0598 0.0579 0.0533};
Params(n,:) = [3.375 0.5 10 200 150 139];
% 20221109 exp2a
Data{n}={'20221109' 'L1750' 0.1758 0.168 0.1838; '20221109' 'blank' 0.0574 0.0604 0.0539};
Params(n,:) = [5.3594 0.5 10 200 150 139];
% 20221109 exp2b
Data{n}={'20221109' 'L2000' 0.1969 0.2161 0.2377; '20221109' 'blank' 0.0574 0.0604 0.0539};
Params(n,:) = [8 0.5 10 200 150 139];
% 20221123 exp1
Data{n}={'20221123' 'Gyroid' 0.3727 0.3882 0.4044; '20221123' 'blank' 0.0524 0.0547 0.0517};
Params(n,:) = [1.7956 0.5 10 200 150 139];

%%%% REACTOR DATA %%
%20220518 R1
DataR{n}={'20220518' 't24p24' 0.0756 0.0781 0.0767; '20211022' 'blank' 0.0512 0.0516 0.0504};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220518 R2
DataR{n}={'20220518' 't24p24' 0.0905 0.0895 0.0881; '20211022' 'blank' 0.05 0.0525 0.0504};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220518 R3
DataR{n}={'20220518' 't24p24' 0.0966 0.0989 0.0973; '20211022' 'blank' 0.0498 0.0521 0.0516};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220518 R4
DataR{n}={'20220518' 't24p24' 0.1099 0.1086 0.1083; '20211022' 'blank' 0.0523 0.0496 0.0497};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220518 R5
DataR{n}={'20220518' 't24p24' 0.1415 0.1405 0.1398; '20211022' 'blank' 0.0514 0.05 0.0505};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 R6
DataR{n}={'20220519' 't24p24' 0.1274 0.1224 0.1255; '20211022' 'blank' 0.0572 0.0515 0.051};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 R7
DataR{n}={'20220519' 't24p24' 0.1219 0.1241 0.1207; '20211022' 'blank' 0.0566 0.0546 0.0521};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 R8
DataR{n}={'20220519' 't24p24' 0.1262 0.1226 0.1216; '20211022' 'blank' 0.0526 0.0518 0.0535};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 R9
DataR{n}={'20220519' 't24p24' 0.1396 0.1395 0.1385; '20211022' 'blank' 0.0541 0.0513 0.0533};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsR(n,:) = [5.9756 0.5 te 200 150 139];

%%%% REACTOR FLOW DATA %%
%20220519 - 25ul/min
DataRF{n}={'20220519' 't24p24' 0.1845 0.1823 0.184; '20211022' 'blank' 0.052 0.0522 0.0517};
te = 500/25;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsRF(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 - 50ul/min
DataRF{n}={'20220519' 't24p24' 0.1396 0.1396 0.1385; '20211022' 'blank' 0.0541 0.0513 0.0533};
te = 500/50;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsRF(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 - 250ul/min
DataRF{n}={'20220519' 't24p24' 0.1003 0.103 0.1026; '20211022' 'blank' 0.0518 0.056 0.0525};
te = 500/250;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsRF(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 - 500ul/min
DataRF{n}={'20220519' 't24p24' 0.0905 0.0933 0.0921; '20211022' 'blank' 0.0533 0.0526 0.052};
te = 500/500;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsRF(n,:) = [5.9756 0.5 te 200 150 139];
%20220519 - 1000ul/min
DataRF{n}={'20220519' 't24p24' 0.0928 0.0946 0.0979; '20211022' 'blank' 0.0518 0.0518 0.0516};
te = 500/1000;%500ul/flow rate(ul/min) = experiment tim (min)
ParamsRF(n,:) = [5.9756 0.5 te 200 150 139];